SELECTIVE REMOVAL OF HEAVY METALS FROM COMPLEX INDUSTRIAL EFFLUENTS BY pH-REGULATED HYDROXIDE PRECIPITATION
DOI:
https://doi.org/10.55640/Keywords:
heavy metals, industrial wastewater, neutralization, hydroxide precipitation, metal removal efficiency, coprecipitation, resource-efficient treatment.Abstract
Industrial wastewater from chemical and metallurgical processes contains high levels of heavy metals, creating serious environmental challenges. This study evaluates pH-controlled neutralization combined with hydroxide precipitation for treating such wastewater. Samples from various production units were analyzed using ICP-OES and XRF before and after treatment. Neutralization at pH 6.5–8.5 enabled the formation of poorly soluble metal hydroxides. Results showed significant reductions in Cu, Zn, Fe, Ni, Pb, and Cd concentrations. Copper and iron dominated the solid phase, while iron hydroxides enhanced removal via coprecipitation and adsorption. Removal efficiencies above 90% were achieved for the most toxic metals. SEM-EDS analysis confirmed stable Cu–Zn–Fe hydroxide phases in residues. The method reduces environmental risks and concentrates valuable metals into a recoverable solid form, supporting resource-efficient wastewater treatment and sustainable water management.
Downloads
References
1.M.N. Abdukodyrova, M.V. Radkevich, K.B. Shipilova. Sewerage and Wastewater Treatment / study guide / Tashkent Institute of Irrigation and Agricultural Mechanization Engineers (TIIAME), 2021, 236 p. https://staff.tiiame.uz/storage/users/606/books/W4gnf0YxayadwUyCyUZSBwEjg9JkIKDvrhfHLZ8A.pdf
2.https://www.vo-da.ru/articles/ochistnye-himicheskih-predpriyatiy/metody-ochistki
3.Гончарук В. В. Вода: проблемы устойчивого развития цивилизации в ХХI веке // Химия и технология воды. – 2004. – T.26, №1.–С.3-25.
4.Воробьев А. В., Каргинов К.Г., Ананикян С.А., Одинцова Е. С. Оценка воздействия на окружающую среду предприятий горной промышленности // Экологическая экспертиза. -2002.- №3.–С.96-104.
5.Трубецкой К.Н., Галченко Ю.П. Человек и природа: противоречия и пути их преодоления // Вестник Российской академии наук. –2002. Т. 72, № 5. –С. 405–409.
6.Скурлатов Ю.И., Дука Г.Г., Мизити А. Введение в экологическую химию // – М.: Высшая школа, –1994. –400 с.
7.Грушко Я. М. Вредные органические соединения в промышленных сточных водах // – Л.: Химия, 1982. –216 с.
8.Холикулов, Д. Б., Р. И. Нормуротов, and Ф. Э. Ахтамов. "Исследования по извлечению цветных металлов ионной флотацией из сбросных растворов. Горный вестник Узбекистана. 2 (2016): 68-70.
9.Якубов, М. М., et al. "Очистка сточных вод медного производства озоном." Узбекский химический журнал 3 (2018): 35-41.
10.Холикулов Д.Б. Применение метода озонирования для обезвреживания технологических растворов медного производства // Universum: технические науки : электрон. научн. журн. 2020. 12(81). URL: https://7universum.com/ru/tech/archive/item/11109.
11.Kholikulov Doniyor, Khojiev Shokhrukh, Kholbay Khaydaraliev, Boltayev Olmos, Khujayev Tuymurod, Abdiev Orif, Yusupov Abdulaziz. Application of ozone for the treatment of process solutions and wastewater in copper production. International Journal of Mechatronics and Applied Mechanics, 2025, Issue 19, Vol. 1. Pp. 193-197. https://ijomam.com/wp-content/uploads/2025/03/pag.-193-197_APPLICATION-OF-OZONE-FOR-THE-TREATMENT-OF-PROCESS-SOLUTIONS-AND-WASTEWATER-IN-COPPER-PRODUCTION.pdf.
12.Холикулов, Д.Б., Рахмонов Н.М., Кодиров С.И.. "Возможности применения ионной флотации для извлечения металлов из различных растворов. Научные основы и практика переработки руд и техногенного сырья: Матер. междунар. науч.-техн. конф. (г. Екатеринбург, 15-18 апр. 2007 г.). Екатеринбург: Форт-Диалог-Исеть. 2007.
13.Абдурахмонов С.А., Холикулов Д.Б., Пиримов А.П., Нормуротов Р.И., Назаров В.Ф. Статистическая обработка показателей ионной флотации металлов из сернокислых растворов. // Горный вестник Узбекистана, Навойи. 2005. № 4 – С. 67–69.
14.Kholikulov D., Khojiev Sh., Khaydaraliev Kh., Boltayev O., Khujayev T., Abdiev O., Yusupov A. Application of ozone for the treatment of process solutions and wastewater in copper production // International Journal of Mechatronics and Applied Mechanics. – 2025. – T. 1. – № 19. – P. 193-197.
15.Kholikulov D.B., Khojiev Sh.T., Khudoymuratov Sh.J., Karshiboev Sh.B., Mutalibkhonov S.S. Potential–pH Analysis of Selective Separation Conditions of Dysprosium, Molybdenum, and Tellurium Metals from Technogenic Solutions // International Journal of Engineering and Information Systems (IJEAIS). – 2025. – Vol. 9. – № 4. – P. 216–221.
16.Kholiqulov D.B., Samadov A.U., Boltaev O.N., Munosibov Sh.M. About the possibility of extraction of metals from mother solutions processing of copper // International Journal of Advanced Research in Science, Engineering, and Technology. – 2019. – Vol. 6, Iss. 3. – P. 8527–8534.
17.Холикулов Д.Б., Болтаев О.Н., Самадов А.У., Абдурахмонов С. Изучение возможности извлечения никеля из отходов медного производства АО «Алмалыкский ГМК» // Advanced Science: сб. ст. V Междунар. науч.-практ. конф. (г. Пенза, 20 нояб. 2018 г.). – Пенза, 2018. – С. 234.
18.Hojiyev Sh.T., Karshiboyev Sh.B., Xudoymuratov Sh.J., Mutalibxonov S.S. Texnogen eritmalardan noyob metallarni ajratib olish imkoniyatlarini tadqiq etish // Sanoatda raqamli texnologiyalar. – 2025. – Vol. 3. – № 3. – P. 27–33.
19.Khojiev Sh.T., Khaydaraliev K.R., Mutalibkhonov S.S., Khudoymuratov S.J. Chemical kinetics and interfacial electron transfer in the hydrazine reduction of zinc ferrite // Development of Science. – 2025. – Vol. 11, No. 3. – P. 445–454.
20.Samadov A. U., Xoliqulov D. B., Matkarimov S. T. (2018). EXTRACTION IRON AND ITS COMPOUNDS FROM SLAGS BY USING GRAVITATION METHODS. European Science Review, (9–10), 231–234. https://doi.org/10.29013/ESR-18-9.10.1-231-234.
Downloads
Published
Versions
- 2026-01-30 (2)
- 2026-04-09 (1)
Issue
Section
License

This work is licensed under a Creative Commons Attribution 4.0 International License.
Authors retain the copyright of their manuscripts, and all Open Access articles are disseminated under the terms of the Creative Commons Attribution License 4.0 (CC-BY), which licenses unrestricted use, distribution, and reproduction in any medium, provided that the original work is appropriately cited. The use of general descriptive names, trade names, trademarks, and so forth in this publication, even if not specifically identified, does not imply that these names are not protected by the relevant laws and regulations.

Germany
United States of America
Italy
United Kingdom
France
Canada
Uzbekistan
Japan
Republic of Korea
Australia
Spain
Switzerland
Sweden
Netherlands
China
India